Split Sample and Blind Sample Programs
Water Quality Coordinated Split Sample Program
The
Chesapeake Bay Program initiated the Coordinated Split Sample Program (CSSP) in
1988 to assess the comparability of water quality results from Chesapeake Bay
Water Quality Laboratories. The water quality CSSP has three components, Mainstem,
Tidal Tributary, and Fall Line, each representing a different salinity levels
in the watershed. Maryland DNR staff collect and split natural water samples four
times a year on routine mainstem and tributary monitoring cruises. USGS staff
collect Fall Line split samples at the twice per year. In June 1999, CSSP sampling
and data analysis protocol (to be revised) were modified to better estimate inter-laboratory
variability.
Laboratories report split sample results to the EPA Chesapeake
Bay Program Office in Annapolis where they are analyzed, reviewed by quality assurance
staff, and discussed quarterly at Analytical
Methods and QA Workgroup meetings. When there is poor agreement among the
lab results, the group investigates significant differences in methods and recommends
corrective actions.
Documentation:
- Procedures
for Sampling and Analyzing Mainstem and Tributary Split Samples (pdf)
- Electronic
Format for Reporting Water Quality Split Samples (pdf)
- Mainstem Split
Sample Graphs (through MM/YY) (pdf)
- Tidal Tributary Split Sample Graphs
(through MM/YY) (pdf)
- Fall Line Split Sample Graphs (through MM/YY) (pdf)
- Problems
Identified, Action Items, and Resolution (need to develop)
- Chesapeake
Bay Program Mainstem Coordinated Split Sample Program Report 1994-1998 (pdf)
Plankton
Split Sample Programs
In 1998, the Chesapeake Bay Program
initiated split sample programs for Phytoplankton, Microzooplankton and Mesozooplankton
to make plankton counts Maryland and Virginia directly comparable. For phytoplankton
and microzooplankton, modifications to existing methods made them comparable but
it was necessary to select a single method for mesozooplankton. Plankton split
samples continue to be collected each year and the Plankton Methods Workgroup
meets once per year to review the results and identify potential differences in
methodologies and taxonomic identifications.
Documentation:
- Procedures
for Counting and Reporting Plankton Split Samples (pdf)
- Format for Reporting
Plankton Split Sample Results (pdf) future online data entry??
- Split Sampling
Study for the Maryland and Virginia Mesozooplankton Monitoring Programs - Final
Report, June 2000 (pdf)
- The 1998 - 1999 Split Sample Study for Chesapeake
Bay Program Phytoplankton & Microzooplankton Monitoring Programs - Final Report,
June 2000 (pdf)
Nutrient and Chlorophyll Blind Audit Samples
The
Chesapeake Bay QA Program also uses low level blind audit samples to check water
quality laboratory performance. The Chesapeake
Biological Laboratory prepares dissolved constituents in artificial seawater,
particulate samples on filter pads, and distribute them twice per year. Each laboratory's
results are compared to the expected values and serve as an external check on
the accuracy of data.
- Chesapeake Bay Program Blind Audit Nutrient
Results - January and June 1998 (pdf)
- Chesapeake Bay Program Blind Audit
Nutrient Results - January and June 1999 (pdf)
- Chesapeake Bay Program
Blind Audit Nutrient Results - January and June 2000 (pdf)
Performance
on USGS Nutrient Reference Samples
Laboratories that
analyze non-tidal water samples in the Chesapeake Bay watershed participate in
the semi-annual USGS
Reference Sample Program. QA staff review the results (Nutrient Reference
Sample Results (pdf)) of Chesapeake Bay laboratories and initiate corrective actions
if necessary.
To
bookmark this page, please use this URL: http://www.chesapeakebay.net/qasample.htm
For
more information, contact the Chesapeake Bay Program Office:
410 Severn Avenue,
Suite 109, Annapolis, MD 21403 / Tel: (800) YOUR-BAY / Fax: (410) 267-5777.
Terms
of Use | Privacy Policy |
Contact Us
Directions to the Bay Program Office


Last modified: 02/12/02
|  |  |