This listing of parameters and method descriptions pertains to the current method codes. To review the complete table of all methods used throughout the program, see
www.chesapeakebay.net/data/index.htm. The first character in the CBP METHOD denotes whether the value is Calculated, measured in the Field, or measured in the Laboratory.
PARAMETER NAME: BIOSI, particulate biogenic silica
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: Particulates collected on a 0.4 um polycarbonate
filter undergo a mild digestion using 0.2 N NAOH. Silicon is analyzed colorimetrically using an
automated silicomolybdate method at a wave length of 660 or 810 nm.
REFERENCE: Technicon Industrial Method No.186-72W, Silicates in Water and Seawater,
(1973)
PARAMETER NAME: BOD5F, 5-day biochemical oxygen demand (filtered)
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 405.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020
PARAMETER NAME: BOD5W, 5-day biochemical oxygen demand (whole)
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 405.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020
PARAMETER NAME: CHLA, chlorophyll a, monochromatic, spectrophotometric
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: APHA - 1002G.
REFERENCE: APHA, 1985. Standard Methods, 16th edition, Method 1002G.
PARAMETER NAME: COND, conductivity, in-situ specific conductance at 25 C
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: A calibrated conductivity sensor attached to a
multi-probe sonde is lowered into a water body and allowed to stabilize prior to taking the meter
reading.
REFERENCE:
PARAMETER NAME: DO, dissolved oxygen, in-situ membrane electrode
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: APHA - 4500-O G
REFERENCE: APHA. Standard Methods, 18th Edition.
PARAMETER NAME: DOC, dissolved organic carbon, combustion infrared method
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: APHA - 5310 B
REFERENCE: APHA, 1980. Standard Methods, 14th Edition. 19th Edition (1996): Method
5310 B.
PARAMETER NAME: DOC, dissolved organic carbon, wet oxidation method
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: APHA - 5310 D
REFERENCE: APHA, 1986. Standard Methods, 19th Edition Supplement. Method 5310 D.
PARAMETER NAME: EPAR_S, epar at surface
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: Reference measurement for incident radiation at
surface of the water. Photosynthetically active radiation (PAR) is measured in air using a flat
cosine quantum light sensor (Li-cor, LI-190SA or equivalent) pointed upwards. Units are
micromoles per second per square meter, which equal microeinsteins. One EPAR_S value is
taken as close as possible in time to each underwater value collected.
REFERENCE:
PARAMETER NAME: EPARD_Z, in-situ, downwelling par
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: Photosynthetically active radiation (PAR) is
measured underwater using a flat cosine quantum sensor (Li-cor LI-190SA or equivalent)
pointing up in the water column. An initial underwater light reading is taken at 0.1 meter depth,
then at 0.5 meter increments until a value of approximately 10 micromoles per second per square
meter is obtained.
REFERENCE:
PARAMETER NAME: FCOLI, fecal coliform, EC medium, MPN
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: APHA - 908 C
REFERENCE: APHA, 1985. Standard Methods, 16th Edition, Method 908 C.
PARAMETER NAME: FCOLI, fecal coliform, direct test, A-1 medium
CBP METHOD: L03
EPA METHOD OR OTHER DESCRIPTION: APHA - 9221 E
REFERENCE: APHA, 1985. Standard Methods, 16th Edition, Method 908 C.
PARAMETER NAME: FSS, fixed suspended solids
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 160.4
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 160.4.
PARAMETER NAME: FSSED, fixed suspended sediment
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: The filter and residue obtained from the
determination of total suspended sediment is ignited at 550 +/- 50 degrees centigrade in a muffle
furnace. The final weight of the residue in mg/l is the fixed suspended sediments (FSSED).
REFERENCE: Fishman and Friedman, 1985. Methods for Determination of Inorganic
Substances in Water and Fluvial Sediments. TWRI-USGS, Book 5, Chapter C1, Laboratory
Theory and Methods for Sediment Analysis, PP.11-18 USGS, Denver Colorado, 1985.
PARAMETER NAME: HARDNESS, titrimetric, EDTA
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: 130.2
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 130.2
PARAMETER NAME: HARDNESS, colorimetric, automated EDTA
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 130.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 130.1
PARAMETER NAME: NH4F, ammonia nitrogen, (filtered), colorimetric, automated phenate
(indophenol)
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 350.1
REFERENCE: A. EPA, 1983. USEPA-600/4-79-020. Method 350.1.
B. EPA, 1993. EPA/600/R-93/100. Method 350.1, Rev 2.
PARAMETER NAME: NH4F, ammonia nitrogen, (filtered), colorimetric, auto
salicylate-hypochlorite
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: Ammonia in a filtered sample reacts with sodium salicylate, sodium nitroprusside and sodium hypochlorite in an alkaline medium to form an intensely colored compound. The resulting color is directly proportional to the concentration of ammonia present. The solution''s color is intensified by sodium nitroprusside, heated and read colorimetrically using an autoanalyzer.
REFERENCE: Fishman and Friedman, 1985. Methods for Determination of Inorganic
Substances in Water and Fluvial Sediments. Techniques of water-resources Investigations of the United States Geological Survey, Book 5, Chapter A1, Denver Colorado, 1985. Method 1-2522-85.
PARAMETER NAME: NH4W, ammonia nitrogen, (whole), colorimetric, automated phenate
(indophenol)
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 350.1
REFERENCE: A. EPA, 1983. USEPA-600/4-79-020. Method 350.1.
B. EPA, 1993. EPA/600/R-93/100. Method 350.1, Rev 2.
PARAMETER NAME: NO23F, nitrite plus nitrate nitrogen (filtered), colorimetric, automated
cadmium reducti
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 353.2
REFERENCE: A. EPA, 1983. USEPA-600/4-79-020. Method 353.2.
B. EPA, 1993. EPA/600/R-93/100. Method 353.2, Rev 2.
PARAMETER NAME: NO23W, nitrite plus nitrate nitrogen, (whole), colorimetric, automated
cadmium reduci
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 353.2
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 353.2.
PARAMETER NAME: NO2F, nitrite nitrogen (filtered), automated, colorimetric, diazotization
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 353.2
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 353.2.
PARAMETER NAME: NO2W, nitrite nitrogen (whole), automated, colorimetric, diazotization
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 353.2
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 353.2.
PARAMETER NAME: PC, particulate carbon
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 440.0
REFERENCE: Methods for the Determination of Chemical Substances in Marine and Estuarine
Matrices. 2nd Edition, 1997. Method 440.0.
PARAMETER NAME: PH, in-situ electrode method
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: 150.1, A calibrated pH electrode, (corrects for
temperature) attached to a multi-probe sonde, is lowered into a water body and allowed to stabilize prior to taking the meter reading.
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 150.1.
PARAMETER NAME: PH, electrode method
CBP METHOD: F02
EPA METHOD OR OTHER DESCRIPTION: 150.1, A grab sample is collected and measured in the field using a portable PH meter (temperature corrected).
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 150.1.
PARAMETER NAME: PHEO, monochromatic, spectrophotometric
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: APHA - 10200 H
REFERENCE: APHA, 1995. Standard Methods, 19th Edition, Method 10200 H.
PARAMETER NAME: PN, particulate nitrogen
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 440.0
REFERENCE: EPA, 1997. 2nd Edition. Method 440.0
PARAMETER NAME: PO4F, orthophosphate, (filtered), automated, ascobic acid
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 365.1, 365.5
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.1.
EPA, 1993. EPA/600/R-93/100. Method 365.1, Rev 2.
EPA, 1997. 2nd Edition, EPA/600/R-97/072, Method 365.5
PARAMETER NAME: PO4W, (whole), orthophosphate, automated, ascobic acid
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 365.1, 365.5
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.1.
EPA, 1993. EPA/600/R-93/100. Method 365.1, Rev 2.
EPA, 1997. 2nd Edition, EPA/600/R-97/072, Method 365.5
PARAMETER NAME: PP, particulate phosphorus, semi-automated, direct
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: Particulates on a 0.7um glass fiber filter are
weighed, then combusted @ 550C to convert organically bound phosphorus to phosphate. Phosphate is extracted with HCL and measured by the automated ascorbic acid method for PO4.
REFERENCE: Aspila, Agemian and Chau, 1976. ''A Semi-automated
Method for the Determination of Inorganic, organic and Total Phosphate in Sediments'', Analyst 101:187-197.
PARAMETER NAME: SALINITY, in-situ measurment
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: In-situ measurement with probe
REFERENCE:
PARAMETER NAME: SECCHI, 20 cm secchi disk
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: A 20 cm diameter secchi disk is lowered into the water and the depth (in meters) at which the black and white quadrants can no longer be distinguished is averaged with the depth at which the black and white quadrants can again be distinguised.
REFERENCE: Tyler, John. 1968. The Secchi Disk, Limnology and Oceanography, 13(1):1-6.
PARAMETER NAME: SIF, silica as SI, (filtered), colorimetric, automated, molybdenum blue
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 366.0
REFERENCE: Methods for the Determination of chemical Substances in Marine and Estuarine Matrices - 2nd Edition, 1997. Method 366.0 ''Dissolved Silicate in Estuarine and Coastal Waters''.
PARAMETER NAME: TALK, alkalinity, titrimetric, ph 4.5
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 310.1
REFERENCE: EPA, 1983, USEPA-600/4-79-020. Method 310.1.
PARAMETER NAME: TCOLI, total coliforms, standard fermemtation technique (MPN)
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: APHA - 908 A
REFERENCE: APHA, 1985. Standard Methods, 16th Edition. Method 908 A.
PARAMETER NAME: TDN, total dissolved nitrogen, alkaline persulfate wet oxidation + EPA
353.2
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: Pre-filtered samples are run through an alkaline
persulfate wet oxidation to change all N-containing compounds into nitrate. Nitrate
concentration is determined using an auto analyzer equipped with a cadmium reduction column.
REFERENCE: D''Elia, C.F., P.A. Steudler and N. Corwin, 1977. ''Determination of Total
Nitrogen in Aqueous Samples using Persulfate Digestion. Limnology and Oceanography,
22:760-764
PARAMETER NAME: TDP, total dissolved phosphorus, alkaline persulfate wet oxidation +
EPA 365.1
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: Filtered samples are run through an alkaline
persulfate wet oxidation, which turns acidic and changes all P-containing compounds into
phosphate. Phosphorus is measured as PO4 using EPA 365.1, an automated spectrophotometric method.
REFERENCE: D''Elia, C.F., P.A. Steudler and N. Corwin, 1977. ''Determination of Total
Nitrogen in Aqueous Samples using Persulfate Digestion. Limnology and Oceanography,
22:760-764
PARAMETER NAME: TDP, total dissolved phosphorus, colorimetric, automated, ascorbic acid
CBP METHOD: L04
EPA METHOD OR OTHER DESCRIPTION: 365.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.1
PARAMETER NAME: TDP, total dissolved phosphorus, block digestor, automated AAII
CBP METHOD: L05
EPA METHOD OR OTHER DESCRIPTION: 365.4
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.4.
PARAMETER NAME: TKNF, total Kjeldahl nitrogen (filtered), semi-automated block digestor, colorimetric, nitro
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: 351.2
REFERENCE: EPA, 1983. USEPA-600/4-79-002. Method 351.2.
PARAMETER NAME: TKNW, total Kjeldahl nitrogen (whole), semi-automated block digestor, colorimetric, nitro
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: 351.2
REFERENCE: EPA, 1983. USEPA-600/4-79-002. Method 351.2.
PARAMETER NAME: TOC, total organic carbon, combustion infrared
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 415.1
REFERENCE: EPA, 1983. USEPA-600/4-79-002. Method 415.1.
PARAMETER NAME: TOC, total organic carbon, wet oxidation
CBP METHOD: L02
EPA METHOD OR OTHER DESCRIPTION: APHA - 5310 D
REFERENCE: APHA, 1996. Standard Methods, 19th Edition Supplement, Method 5310 D.
PARAMETER NAME: TP, total phosphorus, colorimetric, automated, block digestor AAII
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 365.4
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.4.
PARAMETER NAME: TP, total phosphorus, colorimetric, automated, ascorbic acid
CBP METHOD: L04
EPA METHOD OR OTHER DESCRIPTION: 365.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 365.1.
PARAMETER NAME: TSS, total suspended solids, gravimetric, dried at 103-105 C
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 160.2
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 160.2.
PARAMETER NAME: TSSED, total suspended sediment, gravimetric, filtration, dried at 104 C
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: An entire water sample is filtered through one or more 0.45 um membrane filters. The filter(s) and residue are dried at 104 C. Weighing is done on an analytical balance. Filters (clean and with residue) are stored in a dessicator prior to weighing.
REFERENCE: Fishman and Friedman, 1985. Methods for Determination of Inorganic
Substances in Water and Fluvial Sediments. TWRI-USGS, Book 5, Chapter C1, Laboratory Theory and Methods for Sediment Analysis, PP. 11-18. USGS, Denver Colorado, 1985.
PARAMETER NAME: TURB_NTU, turbidity, nephelometric method
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 180.1
REFERENCE: EPA, 1993. EPA/600/R93/100, Method 180.1, Rev 2.
PARAMETER NAME: VSS, volatile suspended solids, gravimetric, ignition at 550 C
CBP METHOD: L01
EPA METHOD OR OTHER DESCRIPTION: 160.4
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 160.4
PARAMETER NAME: WTEMP, water temperature, in-situ
CBP METHOD: F01
EPA METHOD OR OTHER DESCRIPTION: 170.1
REFERENCE: EPA, 1983. USEPA-600/4-79-020. Method 170.1